1SX4
GroEL-GroES-ADP7
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 255.260, 265.250, 184.400 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.000 - 3.000 |
R-factor | 0.259 |
Rwork | 0.258 |
R-free | 0.28730 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.024 |
RMSD bond angle | 2.034 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR |
Refinement software | REFMAC (refmac_5.1.19) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 40.000 |
High resolution limit [Å] | 3.000 |
Number of reflections | 241858 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 298 | PEG 3000, cacodylic acid, sodium glutamate, pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 298 | PEG 3000, cacodylic acid, sodium glutamate, pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |