1SUR
PHOSPHO-ADENYLYL-SULFATE REDUCTASE
Experimental procedure
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID2 |
Synchrotron site | ESRF |
Beamline | ID2 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1996-06 |
Detector | MARRESEARCH |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 82.740, 95.760, 109.800 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 2.000 |
R-factor | 0.19 |
Rwork | 0.190 |
R-free | 0.23000 |
Structure solution method | MIR |
RMSD bond length | 0.011 |
RMSD bond angle | 22.400 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASES |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 10.000 |
High resolution limit [Å] | 1.900 |
Rmerge | 0.081 |
Total number of observations | 129757 * |
Number of reflections | 29105 |
Completeness [%] | 87.4 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 8 * | 4 * | pH 6.0 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 8 (mg/ml) | |
2 | 1 | drop | Tris | 10.0 (mM) | |
3 | 1 | drop | EDTA | 0.1 (mM) | |
4 | 1 | drop | octyl glycoside | 0.25 (%) | |
5 | 1 | reservoir | mPEG5000 | 10 (%(w/v)) | |
6 | 1 | reservoir | calcium acetate | 200 (mM) | |
7 | 1 | reservoir | dithiothreitol | 1 (mM) |