1SUP
SUBTILISIN BPN' AT 1.6 ANGSTROMS RESOLUTION: ANALYSIS OF DISCRETE DISORDER AND COMPARISON OF CRYSTAL FORMS
Experimental procedure
Spacegroup name | C 1 2 1 |
Unit cell lengths | 66.560, 54.150, 62.730 |
Unit cell angles | 90.00, 91.87, 90.00 |
Refinement procedure
Resolution | 8.000 * - 1.600 |
R-factor | 0.17 * |
RMSD bond length | 0.020 |
RMSD bond angle | 0.034 |
Refinement software | PROLSQ |
Data quality characteristics
Overall | |
Number of reflections | 26328 |
Completeness [%] | 92.0 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 7.5 (mg/ml) | |
2 | 1 | drop | MES | 20 (mM) | pH7.0 |
3 | 1 | drop | PMSF | 2 (mM) | |
4 | 1 | reservoir | ammonium sulfate | 35-40 (%saturated) | |
5 | 1 | reservoir | PEG8000 | 0.5 (%) | |
6 | 1 | reservoir | beta-octylglucoside | 1 (%) | |
7 | 1 | reservoir | MPD | 2 (%) | |
8 | 1 | reservoir | MES | 50 (mM) | pH7.0 |