Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL41XU |
| Synchrotron site | SPring-8 |
| Beamline | BL41XU |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 1998-12-03 |
| Detector | MAR CCD 165 mm |
| Wavelength(s) | 0.80 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 165.890, 64.340, 147.140 |
| Unit cell angles | 90.00, 98.08, 90.00 |
Refinement procedure
| Resolution | 15.000 - 2.400 |
| R-factor | 0.246 |
| Rwork | 0.246 |
| R-free | 0.28300 |
| Structure solution method | MULTIPLE ISOMORPHOUS REPLACEMENT USING ANOMALOUS SIGNALS FROM HEAVY ATOMS |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.300 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | MLPHARE |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 2.460 |
| High resolution limit [Å] | 2.400 | 2.400 |
| Rmerge | 0.055 | |
| Number of reflections | 57973 | |
| <I/σ(I)> | 35.06 | 2.9 |
| Completeness [%] | 95.9 | 69 |
| Redundancy | 9 | 2.25 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | MICRODIALYSIS | 6.1 | Sodium butylate, pH 6.10, MICRODIALYSIS | |
| 1 | MICRODIALYSIS | 6.1 | Sodium butylate, pH 6.10, MICRODIALYSIS |
