1STM

SATELLITE PANICUM MOSAIC VIRUS

Experimental procedure

Detector technology	AREA DETECTOR
Collection date	1994-01-01
Detector	SDMS
Spacegroup name	P 42 3 2
Unit cell lengths	183.000, 183.000, 183.000
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	30.000 - 1.900
R-factor	0.21
Rwork	0.210
RMSD bond length	0.014
RMSD bond angle	28.700 *
Data reduction software	SDMS
Data scaling software	SDMS
Phasing software	X-PLOR (3.1)
Refinement software	X-PLOR (3.1)

Data quality characteristics

	Overall
High resolution limit [Å]	1.900 *
Rmerge	0.119 *
Total number of observations	1788746 *
Number of reflections	82620
<I/σ(I)>	1
Completeness [%]	98.0
Redundancy	16

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, sitting drop *		4 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	ammonium salfate	30 (%sat)
2	1	drop	virus solution	10 (mg/ml)
3	1	drop	potassium phosphate	20 (mM)
4	1	drop	ammonium salfate	30 (%sat)