1STF

THE REFINED 2.4 ANGSTROMS X-RAY CRYSTAL STRUCTURE OF RECOMBINANT HUMAN STEFIN B IN COMPLEX WITH THE CYSTEINE PROTEINASE PAPAIN: A NOVEL TYPE OF PROTEINASE INHIBITOR INTERACTION

Experimental procedure

Spacegroup name	P 31 2 1
Unit cell lengths	67.000, 67.000, 169.300
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	8.000 - 2.370
R-factor	0.19 *
Rwork	0.190
RMSD bond length	0.014
RMSD bond angle	2.100
Refinement software	EREF

Data quality characteristics

	Overall	Outer shell
High resolution limit [Å]	2.370 *	2.370 *
Rmerge	0.102 *
Number of reflections	16084 *
Completeness [%]	89.0 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	PEG1550	10 (%)
2	1	reservoir	phosphate	0.75 (M)