1SPE
SPERM WHALE NATIVE CO MYOGLOBIN AT PH 4.0, TEMP 4C
Experimental procedure
| Temperature [K] | 277 |
| Detector technology | AREA DETECTOR |
| Collection date | 1992-12-31 |
| Detector | SIEMENS X1000 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 64.817, 30.756, 35.186 |
| Unit cell angles | 90.00, 106.39, 90.00 |
Refinement procedure
| Resolution | 5.000 - 2.000 |
| R-factor | 0.173 |
| Rwork | 0.173 |
| RMSD bond length | 0.017 |
| RMSD bond angle | 22.330 * |
| Data reduction software | XDS |
| Phasing software | X-PLOR (3.1) |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 30.000 |
| High resolution limit [Å] | 2.000 |
| Rmerge | 0.069 |
| Number of reflections | 7936 |
| Completeness [%] | 86.0 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 4 | pH 4.0 |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | reservoir | ammonium sulfate | (%sat) |
