1SOO
ADENYLOSUCCINATE SYNTHETASE INHIBITED BY HYDANTOCIDIN 5'-MONOPHOSPHATE
Experimental procedure
Source details | ENRAF-NONIUS |
Temperature [K] | 298 |
Detector technology | DIFFRACTOMETER |
Collection date | 1994-08-27 |
Detector | ENRAF-NONIUS FAST |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 70.500, 70.500, 198.800 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.600 |
R-factor | 0.187 |
Rwork | 0.187 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ade |
RMSD bond length | 0.011 |
RMSD bond angle | 24.410 * |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.700 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.110 | 0.344 |
Number of reflections | 15433 | |
Completeness [%] | 95.1 | 85.1 |
Redundancy | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 7.7 * | 20-25 * | pH 4.7 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 19 (mg/ml) | |
2 | 1 | drop | imidazole | 20 (mM) | |
3 | 1 | drop | succinate | 75 (mM) | |
4 | 1 | drop | 2-mercaptoethanol | ||
5 | 1 | reservoir | PEG3350 | 23-25 (%(w/v)) |