1SLB

X-RAY CRYSTALLOGRAPHY REVEALS CROSSLINKING OF MAMMALIAN LECTIN (GALECTIN-1) BY BIANTENNARY COMPLEX TYPE SACCHARIDES

Experimental procedure

Spacegroup name	C 1 2 1
Unit cell lengths	112.800, 41.600, 110.000
Unit cell angles	90.00, 103.00, 90.00

Refinement procedure

Resolution	6.000 - 2.300
R-factor	0.177
Rwork	0.177
RMSD bond length	0.007
RMSD bond angle	1.400
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.300 *
Rmerge	0.110 *
Total number of observations	59848 *
Number of reflections	21316 *
Completeness [%]	90.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	5.5 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	PEG	20-25 (%)