1SLA

X-RAY CRYSTALLOGRAPHY REVEALS CROSSLINKING OF MAMMALIAN LECTIN (GALECTIN-1) BY BIANTENNARY COMPLEX TYPE SACCHARIDES

Experimental procedure

Spacegroup name	P 63 2 2
Unit cell lengths	106.900, 106.900, 119.100
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	6.000 - 2.450
R-factor	0.2
Rwork	0.200
RMSD bond length	0.007
RMSD bond angle	1.460
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.450 *
Rmerge	0.130 *
Total number of observations	99000 *
Number of reflections	14407 *
Completeness [%]	94.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	PEG	15 (%)