1SE2

STAPHYLOCOCCAL ENTEROTOXIN C2, MONOCLINIC FORM

Experimental procedure

Collection date	1994
Detector	SIEMENS
Spacegroup name	P 1 21 1
Unit cell lengths	43.430, 69.920, 42.220
Unit cell angles	90.00, 90.10, 90.00

Refinement procedure

Resolution	8.000 - 2.700
R-factor	0.196
Rwork	0.196
R-free	0.32000
RMSD bond length	0.016
RMSD bond angle	25.800 *
Data reduction software	XGEN
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
Low resolution limit [Å]	20.000
High resolution limit [Å]	2.700
Rmerge	0.053
Total number of observations	16415 *
Number of reflections	7124
Completeness [%]	85.0
Redundancy	2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	7 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	PEG6000	20 (%)
2	1	reservoir	HEPES	100 (mM)