1SDA
CRYSTAL STRUCTURE OF PEROXYNITRITE-MODIFIED BOVINE CU,ZN SUPEROXIDE DISMUTASE
Experimental procedure
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 93.650, 90.330, 71.650 |
| Unit cell angles | 90.00, 95.10, 90.00 |
Refinement procedure
| Resolution | 6.000 * - 2.500 |
| R-factor | 0.187 |
| Rwork | 0.187 |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.230 |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 2.500 * |
| Rmerge | 0.323 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | protein | 2-7 (mg/ml) | |
| 2 | 1 | drop | MPD | 28 (%) | |
| 3 | 1 | drop | potassium phosphate | 50 (mM) | |
| 4 | 1 | reservoir | MPD | 55 (%(v/v)) | |
| 5 | 1 | reservoir | potassium phosphate | 50 (mM) |
