1SD5
Crystal structure of Rv1626
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | EMBL/DESY, HAMBURG BEAMLINE BW7A |
| Synchrotron site | EMBL/DESY, HAMBURG |
| Beamline | BW7A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2003-01-25 |
| Detector | MARRESEARCH |
| Wavelength(s) | 0.981 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 44.558, 44.558, 180.965 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 25.000 - 1.680 |
| R-factor | 0.17302 |
| Rwork | 0.171 |
| R-free | 0.21637 |
| Structure solution method | SAD |
| RMSD bond length | 0.010 |
| RMSD bond angle | 0.947 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | REFMAC (5.1.24) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 40.000 |
| High resolution limit [Å] | 1.680 |
| Number of reflections | 22233 |
| <I/σ(I)> | 32.9 |
| Completeness [%] | 99.9 |
| Redundancy | 11 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | MICROBATCH | 4 | 295 | 15 % PEG 1.5K, pure water, pH 4, Micro Batch, temperature 295K |
