1S8N

Crystal structure of Rv1626 from Mycobacterium tuberculosis

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	EMBL/DESY, HAMBURG BEAMLINE X11
Synchrotron site	EMBL/DESY, HAMBURG
Beamline	X11
Temperature [K]	100
Detector technology	CCD
Collection date	2003-02-20
Detector	MARRESEARCH
Wavelength(s)	0.813
Spacegroup name	P 43 21 2
Unit cell lengths	44.836, 44.836, 180.626
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	30.000 - 1.482
R-factor	0.2042
Rwork	0.203
R-free	0.22835
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1sd5
RMSD bond length	0.009
RMSD bond angle	1.093
Data reduction software	DENZO
Data scaling software	CCP4 ((SCALA))
Phasing software	MOLREP
Refinement software	REFMAC (5.1.24)

Data quality characteristics

	Overall
Low resolution limit [Å]	45.000
High resolution limit [Å]	1.482
Number of reflections	29935
<I/σ(I)>	21.7
Redundancy	6.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	MICROBATCH	4	295	PEG 1.5K, pure water, pH 4, Micro batch, temperature 295K