1RZ0
Flavin reductase PheA2 in native state
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE BM14 |
| Synchrotron site | ESRF |
| Beamline | BM14 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2002-09-12 |
| Detector | MARRESEARCH |
| Wavelength(s) | 0.88570, 0.97917 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 53.544, 154.268, 83.866 |
| Unit cell angles | 90.00, 91.27, 90.00 |
Refinement procedure
| Resolution | 15.000 - 2.200 |
| R-factor | 0.22217 |
| Rwork | 0.222 |
| R-free | 0.25277 |
| Structure solution method | MAD |
| RMSD bond length | 0.017 |
| RMSD bond angle | 1.443 |
| Data scaling software | CCP4 ((SCALA)) |
| Phasing software | SHELXS |
| Refinement software | REFMAC (5.1.27) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 15.000 |
| High resolution limit [Å] | 2.200 |
| Number of reflections | 66610 |
| Completeness [%] | 95.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
