1RYT

RUBRERYTHRIN

Experimental procedure

Detector technology	IMAGE PLATE
Collection date	1994-02-05
Detector	MARRESEARCH
Spacegroup name	I 2 2 2
Unit cell lengths	50.400, 82.000, 100.700
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 - 2.100
R-factor	0.182
Rwork	0.182
R-free	0.25600
RMSD bond length	0.010
RMSD bond angle	1.450 *
Data reduction software	MARXDS
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.100 *
Rmerge	0.050
Number of reflections	11938
Completeness [%]	96.0

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	8 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	TRIZMA hydrochloride	0.1 (M)
2	1	reservoir	PEG1450	15 (%)