1RUJ
RHINOVIRUS 14 MUTANT WITH SER 1 223 REPLACED BY GLY (S1223G)
Experimental procedure
Source type | SYNCHROTRON |
Source details | SRS BEAMLINE PX9.6 |
Synchrotron site | SRS |
Beamline | PX9.6 |
Detector technology | FILM |
Collection date | 1988-06 |
Detector | KODAK |
Wavelength(s) | 0.895 |
Spacegroup name | P 21 3 |
Unit cell lengths | 445.100, 445.100, 445.100 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | ? - 3.000 |
Data reduction software | PURDUE (DATA PROCESSING PACKAGE) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 3.000 |
Rmerge | 0.147 |
Total number of observations | 19491 * |
Number of reflections | 19125 |
Completeness [%] | 4.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 7.2 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | virus | 5 (mg/ml) | |
2 | 1 | drop | PEG8000 | 0.125 (%(w/v)) | or 0.25 %(w/v) |
3 | 1 | drop | Tris-HCl | 0.01 (M) | |
4 | 1 | reservoir | PEG8000 | 0.25 (%(w/v)) | or 0.5 %(w/v) |
5 | 1 | reservoir | 0.02 (M) | ||
6 | 1 | reservoir | Tris-HCl | 0.01 (M) |