1RUD

RHINOVIRUS 14 MUTANT N1105S COMPLEXED WITH ANTIVIRAL COMPOUND WIN 52084

Experimental procedure

Source type	SYNCHROTRON
Source details	CHESS BEAMLINE A1
Synchrotron site	CHESS
Beamline	A1
Detector technology	FILM
Collection date	1990-04
Detector	KODAK
Wavelength(s)	1.563
Spacegroup name	P 21 3
Unit cell lengths	445.100, 445.100, 445.100
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	? - 2.900
Data reduction software	PURDUE (DATA PROCESSING PACKAGE)

Data quality characteristics

	Overall
Low resolution limit [Å]	30.000
High resolution limit [Å]	2.900
Rmerge	0.113
Total number of observations	49305 *
Number of reflections	46561
Completeness [%]	9.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	7.2 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	virus	5 (mg/ml)
2	1	drop	PEG8000	0.125 (%(w/v))	or 0.25 %(w/v)
3	1	drop	Tris-HCl	0.01 (M)
4	1	reservoir	PEG8000	0.25 (%(w/v))	or 0.5%(w/v)
5	1	reservoir		0.02 (M)
6	1	reservoir	Tris-HCl	0.01 (M)