1RPO

RESTORED HEPTAD PATTERN CONTINUITY DOES NOT ALTER THE FOLDING OF A 4-ALPHA-HELICAL BUNDLE

Experimental procedure

Spacegroup name	C 1 2 1
Unit cell lengths	46.960, 37.940, 31.840
Unit cell angles	90.00, 101.04, 90.00

Refinement procedure

Resolution	6.000 - 1.400
R-factor	0.189
Rwork	0.189
RMSD bond length	0.022
RMSD bond angle	0.008 *
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	1.400 *
Rmerge	0.043 *
Number of reflections	10456 *
Completeness [%]	96.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	15 (mg/ml)
2	1	drop	sodium acetate	100 (mM)
3	1	drop	ammonium sulfate	0.8 (M)
4	1	reservoir	ammonium sulfate	1.6 (M)