1RNL
THE NITRATE/NITRITE RESPONSE REGULATOR PROTEIN NARL FROM NARL
Experimental procedure
| Temperature [K] | 277 |
| Detector technology | IMAGE PLATE |
| Collection date | 1995-02-08 |
| Detector | RIGAKU |
| Spacegroup name | I 2 2 2 |
| Unit cell lengths | 61.037, 78.321, 115.720 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 8.000 - 2.400 |
| R-factor | 0.207 |
| Rwork | 0.207 |
| R-free | 0.25100 |
| Structure solution method | MIR |
| RMSD bond length | 0.005 |
| RMSD bond angle | 1.170 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | X-PLOR (3.1) |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 65.000 | 2.440 |
| High resolution limit [Å] | 2.400 | 2.400 |
| Rmerge | 0.071 | |
| Number of reflections | 11188 | |
| <I/σ(I)> | 9.8 | |
| Completeness [%] | 99.9 | 99.3 |
| Redundancy | 5.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
