1RCW
Crystal structure of CT610 from Chlamydia trachomatis
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X12B |
| Synchrotron site | NSLS |
| Beamline | X12B |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2001-06-20 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 0.998, 0.9791, 0.925, 0.9794 |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 77.553, 192.966, 93.740 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 29.880 - 2.500 |
| R-factor | 0.195 |
| Rwork | 0.191 |
| R-free | 0.25800 |
| Structure solution method | MAD |
| RMSD bond length | 0.017 |
| RMSD bond angle | 1.563 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | REFMAC (5.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 29.880 | 2.560 |
| High resolution limit [Å] | 2.500 | 2.500 |
| Number of reflections | 24069 | |
| <I/σ(I)> | 11.2 | 2.3 |
| Completeness [%] | 96.8 | 94.2 |
| Redundancy | 4.1 | 4.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 298 | 10% (v/v) PEG 6K, 20mM cacodylate, pH 6.50, VAPOR DIFFUSION, SITTING DROP, temperature 298K |
