1RCN

CRYSTAL STRUCTURE OF THE RIBONUCLEASE A D(APTPAPAPG) COMPLEX : DIRECT EVIDENCE FOR EXTENDED SUBSTRATE RECOGNITION

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Spacegroup name	P 21 21 21
Unit cell lengths	71.860, 43.200, 43.830
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 - 2.320
R-factor	0.172
Rwork	0.172
RMSD bond length	0.018
RMSD bond angle	3.570
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.300 *
Rmerge	0.129 *
Number of reflections	5664 *
Redundancy	3.9 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	5.3 *	4 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	MPD	51 (%(v/v))
2	1	reservoir	MES	100 (mM)