1RB9
RUBREDOXIN FROM DESULFOVIBRIO VULGARIS REFINED ANISOTROPICALLY AT 0.92 ANGSTROMS RESOLUTION
Experimental procedure
| Source type | SYNCHROTRON |
| Source details | EMBL/DESY, HAMBURG BEAMLINE X31 |
| Synchrotron site | EMBL/DESY, HAMBURG |
| Beamline | X31 |
| Temperature [K] | 293 |
| Detector technology | IMAGE PLATE |
| Collection date | 1988-08 |
| Detector | MARRESEARCH |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 19.970, 41.450, 24.410 |
| Unit cell angles | 90.00, 108.30, 90.00 |
Refinement procedure
| Resolution | 20.000 - 0.920 |
| Structure solution method | MODEL KNOWN (8RXN) |
| Starting model (for MR) | 8rxn |
| RMSD bond length | 0.021 |
| RMSD bond angle | 0.038 |
| Data reduction software | MOSFLM |
| Data scaling software | Agrovata |
| Phasing software | SHELXL-97 |
| Refinement software | SHELXL-97 |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 0.940 |
| High resolution limit [Å] | 0.920 | 0.920 |
| Rmerge | 0.031 | 0.148 |
| Number of reflections | 26124 | |
| <I/σ(I)> | 10 | 3.1 |
| Completeness [%] | 98.5 | 98 |
| Redundancy | 3.7 | 3.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 4.5 | pH 4.5 |
