1RAP

THE STRUCTURE AND FUNCTION OF OMEGA LOOP A REPLACEMENTS IN CYTOCHROME C

Experimental procedure

Spacegroup name	P 43 21 2
Unit cell lengths	36.380, 36.380, 137.630
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	? - 2.250
R-factor	0.183
RMSD bond length	0.018
RMSD bond angle	0.042 *
Refinement software	PROLSQ

Data quality characteristics

	Overall
High resolution limit [Å]	2.250 *
Rmerge	0.073 *
Number of reflections	4498 *
Completeness [%]	86.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	macro-seeding hanging drops *	5.5 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir		95 (%)
2	1	reservoir		0.07 (M)
3	1	reservoir	sodium phosphate	0.1 (M)