1R44
Crystal Structure of VanX
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 17-ID |
| Synchrotron site | APS |
| Beamline | 17-ID |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 1997-10-01 |
| Detector | MARRESEARCH |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 82.597, 44.694, 169.428 |
| Unit cell angles | 90.00, 103.76, 90.00 |
Refinement procedure
| Resolution | 50.000 - 2.250 |
| R-factor | 0.258 |
| Rwork | 0.254 |
| R-free | 0.30100 |
| Structure solution method | MIR |
| RMSD bond length | 0.015 |
| RMSD bond angle | 2.720 |
| Data scaling software | SCALEPACK |
| Phasing software | MLPHARE |
| Refinement software | CNS (0.9) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.300 |
| High resolution limit [Å] | 2.250 | 2.250 |
| Number of reflections | 44765 | |
| Completeness [%] | 79.2 | 75 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.6 | 277 | ammonium sulfate, PEG-monomethyl ester 5000, zinc chloride, pH 7.6, VAPOR DIFFUSION, HANGING DROP, temperature 277.0K |
