Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SRS BEAMLINE PX9.6 |
| Synchrotron site | SRS |
| Beamline | PX9.6 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 1995-07-15 |
| Detector | MARRESEARCH |
| Spacegroup name | I 4 2 2 |
| Unit cell lengths | 102.400, 102.400, 170.500 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 14.600 - 2.500 |
| Rwork | 0.252 |
| R-free | 0.37900 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1aw5 |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.019 |
| Data reduction software | MOSFLM |
| Data scaling software | Agrovata |
| Phasing software | CCP4 |
| Refinement software | CCP4 |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 14.600 | 2.590 |
| High resolution limit [Å] | 2.500 | 2.500 |
| Rmerge | 0.098 | 0.243 |
| Number of reflections | 14956 | |
| <I/σ(I)> | 5.2 | 3 |
| Completeness [%] | 93.0 | 37.6 |
| Redundancy | 6.1 | 2.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 8 | AS FOR PDB ENTRY 1AW5 WITH 1MM LEAD ACETATE, pH 8.00 |
