1QBV
CRYSTAL STRUCTURE OF THROMBIN COMPLEXED WITH AN GUANIDINE-MIMETIC INHIBITOR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | ENRAF-NONIUS FR571 |
Temperature [K] | 288 |
Detector technology | IMAGE PLATE |
Collection date | 1995-05-01 |
Detector | RIGAKU RAXIS II |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 70.900, 71.800, 72.700 |
Unit cell angles | 90.00, 100.52, 90.00 |
Refinement procedure
Resolution | 8.000 - 1.800 |
R-factor | 0.193 |
Rwork | 0.193 |
RMSD bond length | 0.010 |
RMSD bond angle | 26.317 |
Phasing software | X-PLOR |
Refinement software | X-PLOR (98.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 8.000 | 1.880 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.083 * | 0.091 |
Number of reflections | 26244 | |
<I/σ(I)> | 12.2 | |
Completeness [%] | 85.8 | 60.4 |
Redundancy | 5.2 | 2.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.3 | 277.15 | Skrzypczak-Jankun, E., (1991) J. Mol. Biol., 221, 1379. * |