1Q2L

Crystal Structure of pitrilysin

Experimental procedure

Experimental method	MAD
Source type	ROTATING ANODE
Detector technology	IMAGE PLATE
Spacegroup name	P 32 2 1
Unit cell lengths	115.200, 115.200, 178.500
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	12.000 - 2.200
Rwork	0.210
R-free	0.25000
Structure solution method	MAD
RMSD bond length	0.018
RMSD bond angle	1.120
Data reduction software	DENZO
Data scaling software	SCALEPACK
Refinement software	X-PLOR (3.85)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.000
High resolution limit [Å]	2.050	2.050
Number of reflections	98512

Crystallization Conditions

crystal ID	method	pH	temperature	details
1