1Q1P
E-Cadherin activation
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | ELLIOTT GX-21 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2002-12-25 |
Detector | MARRESEARCH |
Wavelength(s) | 1.5418 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 129.204, 48.601, 58.669 |
Unit cell angles | 90.00, 113.93, 90.00 |
Refinement procedure
Resolution | 20.000 - 3.200 |
R-factor | 0.26155 |
Rwork | 0.259 |
R-free | 0.30484 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1FF5.pdb |
RMSD bond length | 0.012 |
RMSD bond angle | 1.877 |
Data reduction software | MOSFLM |
Data scaling software | CCP4 ((SCALA)) |
Phasing software | AMoRE |
Refinement software | REFMAC (5.0) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 37.470 |
High resolution limit [Å] | 3.180 |
Number of reflections | 5324 |
<I/σ(I)> | 8.3 |
Completeness [%] | 99.8 |
Redundancy | 3.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |