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1PY4

Beta2 microglobulin mutant H31Y displays hints for amyloid formations

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsELETTRA BEAMLINE 5.2R
Synchrotron siteELETTRA
Beamline5.2R
Temperature [K]100
Wavelength(s)0.927
Spacegroup nameC 2 2 21
Unit cell lengths105.195, 150.166, 93.671
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution10.000 - 2.900
R-factor0.24084
Rwork0.240
R-free0.31308
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1lds
RMSD bond length0.014
RMSD bond angle1.631
Data reduction softwareMOSFLM
Data scaling softwareCCP4 ((SCALA))
Phasing softwareAMoRE
Refinement softwareREFMAC (5.1.19)
Data quality characteristics
 Overall
Low resolution limit [Å]30.000
High resolution limit [Å]2.900
Number of reflections16354
<I/σ(I)>19.8
Completeness [%]99.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP5.6300PEG 4K 31%, glycerol 25%, ammonium acetate 0.2 M, pH 5.6, VAPOR DIFFUSION, HANGING DROP, temperature 300K
1VAPOR DIFFUSION, HANGING DROP5.6300PEG 4K 31%, glycerol 25%, ammonium acetate 0.2 M, pH 5.6, VAPOR DIFFUSION, HANGING DROP, temperature 300K

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