1PSH
CRYSTAL STRUCTURE OF PHOSPHOLIPASE A2 FROM INDIAN COBRA REVEALS A TRIMERIC ASSOCIATION
Experimental procedure
Spacegroup name | P 43 21 2 |
Unit cell lengths | 88.600, 88.600, 107.400 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 6.000 - 2.300 |
R-factor | 0.174 |
Rwork | 0.174 |
RMSD bond length | 0.013 |
RMSD bond angle | 2.940 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.300 * |
Rmerge | 0.047 * |
Total number of observations | 226069 * |
Completeness [%] | 91.6 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Microdialysis * | 8 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | enzyme | 10 (mg/ml) | |
2 | 1 | 2 | ethanol | 20 (%(v/v)) | |
3 | 1 | 2 | 5 (mM) | ||
4 | 1 | 2 | Tris-HCl | 50 (mM) |