1PPK

CRYSTALLOGRAPHIC ANALYSIS OF TRANSITION STATE MIMICS BOUND TO PENICILLOPEPSIN: PHOSPHOROUS-CONTAINING PEPTIDE ANALOGUES

Experimental procedure

Spacegroup name	C 1 2 1
Unit cell lengths	97.480, 46.550, 66.420
Unit cell angles	90.00, 116.14, 90.00

Refinement procedure

Resolution	8.000 - 1.800
R-factor	0.132
RMSD bond length	0.022
RMSD bond angle	0.044
Refinement software	PROLSQ

Data quality characteristics

	Overall
Low resolution limit [Å]	45.000 *
High resolution limit [Å]	1.800
Rmerge	0.033 *
Total number of observations	29429 *
Number of reflections	24917 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	4.4 *	18-22 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	complex	10 (mg/ml)
2	1	drop	ammonium sulfate	34-40 (%sat)
3	1	drop		0.1 (M)