1PPF

X-RAY CRYSTAL STRUCTURE OF THE COMPLEX OF HUMAN LEUKOCYTE ELASTASE (PMN ELASTASE) AND THE THIRD DOMAIN OF THE TURKEY OVOMUCOID INHIBITOR

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	73.050, 72.550, 52.450
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 - 1.800
R-factor	0.166 *
Rwork	0.166
Refinement software	EREF

Data quality characteristics

	Overall
High resolution limit [Å]	1.700 *
Rmerge	0.083 *
Total number of observations	62000 *
Number of reflections	21000 *
Completeness [%]	75.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	10 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	sodium citrate	0.45-0.5 (M)