1PNN
PEPTIDE NUCLEIC ACID (PNA) COMPLEXED WITH DNA
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | CHESS BEAMLINE A1 |
| Synchrotron site | CHESS |
| Beamline | A1 |
| Detector technology | CCD |
| Collection date | 1994-05-08 |
| Wavelength(s) | 0.978 |
| Spacegroup name | P 65 2 2 |
| Unit cell lengths | 73.380, 73.380, 141.280 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 6.000 - 2.500 |
| R-factor | 0.187 |
| Rwork | 0.187 |
| R-free | 0.23500 |
| RMSD bond length | 0.014 |
| RMSD bond angle | 2.430 |
| Data reduction software | DENZO |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.000 |
| High resolution limit [Å] | 2.500 |
| Rmerge | 0.043 |
| Number of reflections | 8374 |
| Completeness [%] | 93.0 |
| Redundancy | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 8.5 | pH 8.5 | ||
| 1 | 8.5 | pH 8.5 |
