1PK4

CRYSTAL AND MOLECULAR STRUCTURE OF HUMAN PLASMINOGEN KRINGLE 4 REFINED AT 1.9-ANGSTROMS RESOLUTION

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	32.110, 49.090, 49.390
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	? - 1.900
R-factor	0.142
RMSD bond length	0.018
RMSD bond angle	0.044 *
Refinement software	PROFFT

Data quality characteristics

	Overall
High resolution limit [Å]	1.900 *
Rmerge	0.410 *
Number of reflections	4869 *
Completeness [%]	73.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, sitting drop *	6 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	PEG8000	30 (%(w/v))
2	1	reservoir	ammonium sulfate	0.12 (M)
3	1	reservoir	dimethylformamide	1.2 (%)