1PDR

CRYSTAL STRUCTURE OF THE THIRD PDZ DOMAIN FROM THE HUMAN HOMOLOG OF DISCS LARGE PROTEIN

Experimental procedure

Detector technology	IMAGE PLATE
Collection date	1996-04-12
Detector	RIGAKU
Spacegroup name	P 63 2 2
Unit cell lengths	110.970, 110.970, 62.470
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	10.000 - 2.800
R-factor	0.22
Rwork	0.220
R-free	0.27100
RMSD bond length	0.008 *
RMSD bond angle	1.400 *
Data reduction software	DENZO
Phasing software	X-PLOR (3.1)
Refinement software	X-PLOR (3.1)

Data quality characteristics

	Overall	Outer shell
High resolution limit [Å]	2.800 *
Rmerge	0.108	0.301 *
Number of reflections	5911
Completeness [%]	100.0
Redundancy	13

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *		4 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	15 (mg/ml)
2	1	reservoir	sodium citrate	0.9-1.3 (M)