1PAL
IONIC INTERACTIONS WITH PARVALBUMINS. CRYSTAL STRUCTURE DETERMINATION OF PIKE 4.10 PARVALBUMIN IN FOUR DIFFERENT IONIC ENVIRONMENTS
Experimental procedure
Spacegroup name | P 21 21 2 |
Unit cell lengths | 59.500, 59.630, 26.240 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 7.000 * - 1.650 |
R-factor | 0.197 |
RMSD bond length | 0.024 |
RMSD bond angle | 0.064 |
Refinement software | PROLSQ |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 9999.000 * | |
High resolution limit [Å] | 1.650 * | 1.650 * |
Rmerge | 0.101 * | |
Total number of observations | 29643 * | |
Number of reflections | 11782 * | |
Completeness [%] | 74.0 * | 53 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 20 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | sodium azide | 3 (mM) |