1PAL

IONIC INTERACTIONS WITH PARVALBUMINS. CRYSTAL STRUCTURE DETERMINATION OF PIKE 4.10 PARVALBUMIN IN FOUR DIFFERENT IONIC ENVIRONMENTS

Experimental procedure

Spacegroup name	P 21 21 2
Unit cell lengths	59.500, 59.630, 26.240
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	7.000 * - 1.650
R-factor	0.197
RMSD bond length	0.024
RMSD bond angle	0.064
Refinement software	PROLSQ

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	9999.000 *
High resolution limit [Å]	1.650 *	1.650 *
Rmerge	0.101 *
Total number of observations	29643 *
Number of reflections	11782 *
Completeness [%]	74.0 *	53 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *		20 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	sodium azide	3 (mM)