1P2X
CRYSTAL STRUCTURE OF THE CALPONIN-HOMOLOGY DOMAIN OF RNG2 FROM SCHIZOSACCHAROMYCES POMBE
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM14 |
Synchrotron site | ESRF |
Beamline | BM14 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2002-09-15 |
Detector | MARRESEARCH |
Wavelength(s) | 0.919087, 0.919338, 0.855057 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 31.226, 68.836, 39.811 |
Unit cell angles | 90.00, 105.54, 90.00 |
Refinement procedure
Resolution | 22.650 - 2.210 |
R-factor | 0.206 |
Rwork | 0.206 |
R-free | 0.26200 |
Structure solution method | MAD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.000 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHARP |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 22.650 | 2.290 |
High resolution limit [Å] | 2.210 | 2.210 |
Rmerge | 0.053 | 0.077 |
Number of reflections | 7532 | |
<I/σ(I)> | 0.053 | 9.39 |
Completeness [%] | 89.6 | 24.8 |
Redundancy | 3.47 | 2.09 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 295 | 21% PEG 3000, 0.3M Calcium Acetate, 0.1M Tris pH 7, VAPOR DIFFUSION, SITTING DROP, temperature 295K |