1P2P
STRUCTURE OF PORCINE PANCREATIC PHOSPHOLIPASE A2 AT 2.6 ANGSTROMS RESOLUTION AND COMPARISON WITH BOVINE PHOSPHOLIPASE A2
Experimental procedure
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 69.820, 69.820, 67.660 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 7.000 * - 2.600 |
| R-factor | 0.241 * |
| Rwork | 0.241 |
| RMSD bond length | 0.006 * |
| Refinement software | PROLSQ |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 2.600 * |
| Rmerge | 0.058 * |
| Number of reflections | 4603 * |
| Completeness [%] | 74.9 * |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 7.2 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | Tris-maleate | 0.05 (M) | |
| 2 | 1 | 1 | 5 (mM) | ||
| 3 | 1 | 1 | methanol | 0.010-0.015ml |
