1OVO

CRYSTALLOGRAPHIC REFINEMENT OF JAPANESE QUAIL OVOMUCOID, A KAZAL-TYPE INHIBITOR, AND MODEL BUILDING STUDIES OF COMPLEXES WITH SERINE PROTEASES

Experimental procedure

Spacegroup name	P 4 21 2
Unit cell lengths	92.000, 92.000, 64.000
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	6.000 * - 1.900
R-factor	0.207 *
Refinement software	REAL-SPACE (REFINEMENT)

Data quality characteristics

	Overall
High resolution limit [Å]	1.900 *
Rmerge	0.084 *
Total number of observations	63795 *
Number of reflections	19537 *
Completeness [%]	75.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	9.5 *	20 *	Weber, E., (1981) J.Mol.Biol., 149, 109. *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	citrate	0.96-1.0 (M)