1OUT
TROUT HEMOGLOBIN I
Experimental procedure
| Source type | SYNCHROTRON |
| Source details | SRS BEAMLINE PX9.6 |
| Synchrotron site | SRS |
| Beamline | PX9.6 |
| Temperature [K] | 293 |
| Detector technology | IMAGE PLATE |
| Detector | MAR scanner 300 mm plate |
| Spacegroup name | P 65 2 2 |
| Unit cell lengths | 63.280, 63.280, 312.740 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 8.000 - 2.300 |
| R-factor | 0.162 * |
| Rwork | 0.162 |
| R-free | 0.24700 |
| RMSD bond length | 0.014 |
| RMSD bond angle | 0.030 |
| Data reduction software | MOSFLM |
| Refinement software | PROLSQ |
Data quality characteristics
| Overall | |
| Rmerge | 0.049 |
| Number of reflections | 17315 |
| Completeness [%] | 84.9 |
| Redundancy | 4.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 6 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | bis-Tris-HCl | 50 (mM) | |
| 2 | 1 | 1 | PEG8000 | 15 (%) |
