1OPG

OPG2 FAB FRAGMENT

Experimental procedure

Collection date	1992-03-12
Spacegroup name	P 21 21 2
Unit cell lengths	93.100, 83.800, 53.700
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 - 2.000
R-factor	0.16
RMSD bond length	0.017
RMSD bond angle	0.063
Data reduction software	XENGEN ((HOWARD)
Refinement software	PROLSQ

Data quality characteristics

	Overall
High resolution limit [Å]	2.000 *
Rmerge	0.044
Total number of observations	89211 *
Number of reflections	28703
Completeness [%]	99.0
Redundancy	3.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *		22 *	Celikel, R., (1993) Acta Crystallogr.,Sect.D, 49, 421. *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	PEG1000	24 (%(w/v))
2	1	reservoir	imidazole malate	0.02 (M)
3	1	reservoir		0.16 (M)