1OLC

OLIGO-PEPTIDE BINDING PROTEIN (OPPA) COMPLEXED WITH LYS-LYS-LYS-ALA

Experimental procedure

Temperature [K]	291
Detector technology	IMAGE PLATE
Detector	RIGAKU RAXIS IIC
Wavelength(s)	1.5418
Spacegroup name	P 21 21 21
Unit cell lengths	110.730, 77.080, 71.330
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 - 2.100
R-factor	0.143
R-free	0.19700
RMSD bond length	0.018
RMSD bond angle	0.035
Data reduction software	DENZO
Refinement software	PROLSQ

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.000
High resolution limit [Å]	2.000
Rmerge	0.063	0.176 *
Number of reflections	41810
Completeness [%]	99.7	100 *
Redundancy	4.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	5.5		pH 5.5

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	PEG4000	7-10 (%)
2	1	reservoir	sodium acetate	50 (mM)
3	1	reservoir	uranyl acetate	1 (mM)