1OEN
PHOSPHOENOLPYRUVATE CARBOXYKINASE
Experimental procedure
Detector technology | DIFFRACTOMETER |
Collection date | 1991-06-03 |
Detector | ENRAF-NONIUS FAST |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 77.696, 89.660, 93.836 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 6.000 - 1.900 |
R-factor | 0.202 |
Rwork | 0.202 |
R-free | 0.24400 |
RMSD bond length | 0.006 |
RMSD bond angle | 24.610 * |
Data reduction software | MADNES |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.900 * |
Rmerge | 0.093 * |
Total number of observations | 249762 * |
Number of reflections | 47596 * |
Completeness [%] | 90.8 * |
Redundancy | 5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | seeding * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 10 (mg/ml) | |
2 | 1 | drop | Tris-HCl | 20 (mM) | |
3 | 1 | drop | EDTA | 0.1 (mM) | |
4 | 1 | reservoir | sodium acetate | 100 (mM) | |
5 | 1 | reservoir | PEG8000 | 15-20 (%) | |
6 | 1 | reservoir | sodium azide | 0.02 (%(w/v)) |