1OCR
BOVINE HEART CYTOCHROME C OXIDASE IN THE FULLY REDUCED STATE
Experimental procedure
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-6A |
Synchrotron site | Photon Factory |
Beamline | BL-6A |
Temperature [K] | 283 |
Detector technology | IMAGE PLATE |
Collection date | 1996-05-19 |
Detector | FUJI |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 189.100, 210.500, 178.600 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 15.000 - 2.350 |
R-factor | 0.211 * |
Rwork | 0.203 |
R-free | 0.25100 * |
Structure solution method | MULTIPLE ISOMORPHOUS REPLACEMENT |
RMSD bond length | 0.015 |
RMSD bond angle | 25.205 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR (3.84) |
Refinement software | X-PLOR (3.84) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.000 | 2.460 |
High resolution limit [Å] | 2.350 | 2.350 |
Rmerge | 0.062 | 0.320 |
Total number of observations | 1184694 * | |
Number of reflections | 270061 | 28814 * |
<I/σ(I)> | 14.4 | 2 |
Completeness [%] | 89.2 | 72 |
Redundancy | 4.4 | 1.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 6.8 | pH 6.8 |