1OCO
BOVINE HEART CYTOCHROME C OXIDASE IN CARBON MONOXIDE-BOUND STATE
Experimental procedure
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-6A |
Synchrotron site | Photon Factory |
Beamline | BL-6A |
Temperature [K] | 283 |
Detector technology | IMAGE PLATE |
Collection date | 1996-07-21 |
Detector | FUJI |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 189.100, 210.500, 178.600 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 7.000 - 2.800 |
R-factor | 0.213 |
Rwork | 0.213 |
R-free | 0.25600 |
Structure solution method | MULTIPLE ISOMORPHOUS REPLACEMENT |
RMSD bond length | 0.014 |
RMSD bond angle | 26.149 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR (3.84) |
Refinement software | X-PLOR (3.84) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.000 | 2.900 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.062 * | 0.320 * |
Total number of observations | 1656746 * | |
Number of reflections | 173384 | 14954 * |
<I/σ(I)> | 14.7 | 3.5 |
Completeness [%] | 97.5 | 85 |
Redundancy | 9.5 | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 6.8 | pH 6.8 |