1O1R
Structure of FPT bound to GGPP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 1999-11-15 |
Detector | MAR CCD 165 mm |
Spacegroup name | P 61 |
Unit cell lengths | 171.650, 171.650, 69.080 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 8.000 - 2.300 |
R-factor | 0.177 |
Rwork | 0.177 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.380 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.063 | 0.367 |
Number of reflections | 51180 | |
<I/σ(I)> | 24.1 | |
Completeness [%] | 99.3 | 99.9 |
Redundancy | 3.7 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 5.7 | 298 | PEG 4000, Sodium Acetate, KCl, pH 5.7, hanging drop, temperature 298.0K |