1O1L
Deoxy hemoglobin (A-GLY-C:V1M,L29W,H58Q; B,D:V1M)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 295 |
Detector technology | IMAGE PLATE |
Collection date | 2000-03-15 |
Detector | RIGAKU RAXIS IV |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 63.363, 83.185, 53.736 |
Unit cell angles | 90.00, 98.80, 90.00 |
Refinement procedure
Resolution | 8.000 - 1.800 |
R-factor | 0.205 |
R-free | 0.25400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1c7c |
RMSD bond length | 0.005 |
RMSD bond angle | 0.015 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHELX |
Refinement software | SHELXL-97 |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.900 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.074 | 0.275 |
Number of reflections | 47994 | |
<I/σ(I)> | 16.2 | 6.1 |
Completeness [%] | 94.2 | 91.9 |
Redundancy | 2.771 | 2.66 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | pH 6.50 |