1NZR
CRYSTAL STRUCTURE OF THE AZURIN MUTANT NICKEL-TRP48MET FROM PSEUDOMONAS AERUGINOSA AT 2.2 ANGSTROMS RESOLUTION
Experimental procedure
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 57.400, 80.400, 110.300 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 8.000 * - 2.200 |
| R-factor | 0.17 |
| Rwork | 0.170 |
| RMSD bond length | 0.015 |
| RMSD bond angle | 3.130 |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | |
| Rmerge | 0.087 * |
| Total number of observations | 82349 * |
| Number of reflections | 17974 * |
| Completeness [%] | 73.0 * |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 5.7 * | 297-298 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | ammonium sulfate | 3.2 (M) | |
| 2 | 1 | 1 | lithium nitrate | 1.0 (M) | |
| 3 | 1 | 1 | acetate | 0.2 (M) |
