1NSD
INFLUENZA B VIRUS NEURAMINIDASE CAN SYNTHESIZE ITS OWN INHIBITOR
Experimental procedure
Spacegroup name | P 31 2 1 |
Unit cell lengths | 88.900, 88.900, 222.800 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | ? - 1.800 |
R-factor | 0.169 |
Rwork | 0.169 |
RMSD bond length | 0.013 |
RMSD bond angle | 2.860 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.800 * |
Rmerge | 0.090 * |
Total number of observations | 101118 * |
Number of reflections | 62852 * |
Completeness [%] | 66.0 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Batch method * | 7.9 * | taken from Burmeister, W.P. et al (1992). Embo J., 11, 49-56. * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | protein | 6 (mg/ml) | |
2 | 1 | 1 | PEG4000 | 5 (%) | |
3 | 1 | 1 | 75 (mM) | ||
4 | 1 | 1 | phosphate | 60 (mM) |